RG25/50/75/120

Our RHEOGRAPHES 25, 50, 75 and 120 are user-friendly high-pressure capillary rheometers with a further extended shear rate range, higher test load (25, 50, 75 and 120 kN) and a wide range of add-ons.

  • ISO 17744 (PVT)
  • ASTM D5930 (TCM)
  • ASTM D5099 (Gummi)
  • ISO 11443 (Viskosität)
  • ASTM D3835 (Viskosität)

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Capillary Rheometer RG25-120

Increased shear rate range

The series of GÖTTFERT high pressure capillary rheometers is available with different test loads of 25, 50, 75 or 120 kN. The stronger versions such as RG75 or RG120 can achieve extremely high shear rates even with very high viscosity test material. Due to a unique and large variety of modular add-ons not otherwise available on the market, other material properties can be tested in addition to viscosity. It is possible to characterize all process-relevant material behaviors.

Good to know

All high-pressure capillary rheometers of this series are available as single-, twin- or triple-barrel versions with different test barrel diameters. We also offer a large number of capillaries and other options that make it possible to adapt the machine perfectly to your application.




Specification

Product features

  • Maximum test force of 25, 50, 75 or 120 kN
  • Single- or multi-barrel system
  • Barrel diameter 9.55, 12, 15, 20, 25 or 30 mm, others on request
  • Dynamic speed range 0.00004 - 40 mm/s (1:1000000)
  • High dynamic acceleration of the test pistion (from 0 to 40 in 0.6 seconds)
  • Piston position measurement with high-resolution encoder
  • Adaptive signal resolution of only 0.005 % from the pressure transducer range
  • Temperature up to 400°C (500°C optional)
  • Alternative steel grades for barrel and piston with higher corrosion or abrasion resistance
  • Optional: Isothermal or isobaric PVT-measurements
  • Optional: Innovative air-cooling system, cooling rate max. 30 K/min

CUSTOMIZED TO YOUR REQUIREMENTS

Add-ons for advanced measurements

Our modular add-ons also offer an extended option for characterizing materials.

Measuring first normal stress difference at high shear rates via capillary rheometer.

  • Determination of Normal Stress at high shear rates and closer to the processing shear rates which was not possible with conventional technique​
  • Detection of flow instabilities at processing shear rates​
  • Measurement of Viscosity, elongation viscosity and Normal Stress differences​

 

PVT(等温/等压)

除了PVT500以外,高特福还提供可以做为毛细管流变仪附加组件的测试单元来来测试PVT,该测量可以表征材料温度,比体积和压力之间的特性关系。

 

  • 根据ISO 17744来进行等压或等温测试
  • 新开发的高效气冷冷却器和恒温器
  • 全自动测量
  • 自动生成PVT图
  • 获得Tait模型的参数来和相应的仿真软件建立联系。
HAUL-OFF熔体强度测试仪

我们新开发的最大速度可以达到2000m/min的牵引装置特别适合于纤维级材料的特性描述,此系统可以以一个恒定加速度的或者分步恒速的模式来运行,通过一个平稳运行,有防粘涂层的滚轮来提供拉力,滚轮和一个高灵敏度的力传感器连接。

 

Rheotens熔体拉伸流变仪

在塑料的生产和加工过程中,聚合物熔体的拉伸性能是至关重要的。

已经获得专利的RHEOTENS 方法被证实是一种极其灵敏的测量原理,能够提供高重复性的测试结果,甚至可以显示最小的批次波动。

除了已经具有的恒速和恒定加速的模式外,现在还具有指数加速度的模式,根据Wagner教授的说法,拉伸粘度函数的确定是RHEOTHENS不可或缺的一部分。

RHEOTENS非常适合对一些挤出或成膜材料的加工性能进行测试。

Contifeed全自动熔体进料单元

CONTIFEED是一种微型挤出机,直接和毛细管流变仪的料筒相连,由于样品停留的时间缩短,这种附加装置特别适用于热不稳定材料,在挤出机中进行预剪切塑化,使测量过程与生产过程十分接近。

 

CONTIFEED的优点:

  • 自动,无气泡的填充料筒
  • 可以研究挤出塑化的影响
  • 减小材料在温度影响下的停留时间
  • 在与生产过程相似的流动条件下测试流变特性。
  • 预塑化还可以测量粉末材料(例如 PVC干粉料)

El cabezal de medición Shark Skin se monta en la parte inferior del canal en lugar de la boquilla. Con esta opción se puede medir de forma exacta con qué velocidades de cizalla críticas se producen homogeneidades de la superficie.

  • Registro del efecto Shark Skin
  • Formado por la boquilla ranurada, tres nuevos sensores de presión de alta frecuencia (velocidad de muestreo de hasta 20 kHZ) y un paquete de software
  • Determinación de la gama de frecuencias y evaluación estadística de la señal de presión
  • Optimización del proceso de extrusión, de extrusión de película y de revestimiento

 

热导率

热导率传感器的安装方式与标准活塞相同。在实验过程中,料筒的底部是被密封的。固体或者熔体的热导率测量是在相同条件下进行的。

 

  • 测试热导率时最高可以达到450摄氏度和1000bar。
  • 根据ASTM D5930开发。
  • 测试单元包含加热单元和温度传感器。
  • 注塑过程的模拟与周期优化。
  • 无需任何的机械改装。
  • 全自动测量
反向压力测试

聚合物的粘度也取决于全部的压力情况,反向压力测试安装在口模后面,在口模出口处产生一个反向的压力,这个反向的压力由一个附加的压力传感器测量

 

  • 测粘度(压力系数)与压力的相关性
  • 壁滑移临界剪切应力的测定
  • 最大压力(1200)bar
  • 温度最高达400摄氏度
  • 机械加工中流动过程的优化(长管道注塑和挤出,熔体泵)
挤出胀大测试单元

测量头安装在口模下方,口模胀大和粘度测试可以同时进行。

 

  • 动态和静态挤出胀大的测定
  • 挤出胀大曲线的评估(BASELL法)
  • 具有高度调节共亨的旋转壁
  • 0.1微米或者7微米的激光测量头
  • 可以选配自动熔体切割装置
  • 选配:可以同时测量两束熔体柱
  • 应用:模拟材料挤压过程中的膨胀

Best practise

PVT isobaric

This procedure is standardized in ISO 17744 for piston operated instruments. Isobaric PVT measurements are performed at constant pressure...

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PVT isothermal

In isothermal PVT measurement, the measurement process starts at room temperature after the material is filled at melt temperature and...

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Bagley Correction

The Bagley correction is needed to calculate the inlet pressure drop when round hole capillaries...

 

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Weißenberg-Rabinowitsch Correction

Due to shear thinning of polymer melts with pseudoplastic flow behaviour a strong flection of the...

 

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Multi-Load Schmelzindex Messungen

Schmelzindex-Prüfgeräte werden insbesondere in der Qualitätskontrolle von Kunststoffherstellern wie auch Verarbeitern eingesetzt...

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Thermo Stability

Plastics have the property of aging through thermal or mechanical stress...

 

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Melt Elasticity/Strength

The melt strength (elasticity) is determined by withdrawing an extruded strand of capillary rheometer...

 

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Die Swell Measurement

The Die Swell measurement is one of many available add-ons for the series of GOETTFERT capillary rheometers...

 

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Counterpressure chamber

The counter pressure chamber, which offered by GÖTTFERT as an optional Add-on ...

 

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Flow Instabilities (Shark-Skin)

The Shark-Skin effect occurs during the extrusion of plastics, elastomers or food and manifests...

 

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Thermal Conductivity

The measurement of the thermal conductivity is carried out by means of a probe...

 

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Extensional viscosity (Cogswell Modell)

The extensional viscosity can be calculated with measured data of a capillary rheometer...

 

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